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A method for the determination of chlorinated organic compounds in aquatic tissue by dual capillary-column gas chromatography with electron-capture detection is described. Whole-body-fish or corbicula tissue is homogenized, Soxhlet extracted, lipid removed by gel permeation chromatography, and fractionated using alumina/silica adsorption chromatography. The extracts are analyzed by dissimilar capillary-column gas chromatography with electron-capture detection. The method reporting limits are 5 micrograms per kilogram ( | "USGS Publications Warehouse": { | ||
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"name": "Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory; determination of chlorinated pesticides in aquatic tissue by capillary-column gas chromatography with electron-capture detection", | |||
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"value": "ofr94710W", | |||
"url": "https://pubs.usgs.gov/publication/ofr94710W" | |||
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"value": 17338 | |||
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"propertyID": "DOI", | |||
"value": "10.3133/ofr94710W", | |||
"url": "https://doi.org/10.3133/ofr94710W" | |||
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"datePublished": "1995", | |||
"dateModified": "2020-02-26", | |||
"abstract": "A method for the determination of chlorinated organic compounds in aquatic tissue by dual capillary-column gas chromatography with electron-capture detection is described. Whole-body-fish or corbicula tissue is homogenized, Soxhlet extracted, lipid removed by gel permeation chromatography, and fractionated using alumina/silica adsorption chromatography. The extracts are analyzed by dissimilar capillary-column gas chromatography with electron-capture detection. The method reporting limits are 5 micrograms per kilogram (\u03bcg/kg) for chlorinated compounds, 50 \u03bcg/kg for polychlorinated biphenyls, and 200 \u03bcg/kg for toxaphene.", | |||
"description": "v, 42 p.", | |||
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"name": "U.S. Geological Survey" | |||
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"name": "Leiker, Thomas J.", | |||
"givenName": "Thomas J.", | |||
"familyName": "Leiker" | |||
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"name": "Deacon, Jeffrey R. jrdeacon@usgs.gov", | |||
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"name": "National Water Quality Program", | |||
"url": "https://www.usgs.gov/programs/national-water-quality-program" | |||
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"@type": "Organization", | |||
"name": "National Water Quality Assessment Program", | |||
"url": "https://www.usgs.gov/programs/national-water-quality-program" | |||
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"name": "NH/VT office of New England Water Science Center", | |||
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"name": "Foreman, William T. wforeman@usgs.gov", | |||
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