Item talk:Q240685
From geokb
{
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"name": "Bobjonesite, V4+ O (SO4) (H2O)3, a new mineral species from Temple Mountain, Emery County, Utah, U.S.A",
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"abstract": "Bobjonesite, V4+\u00a0O (SO4) (H2O)3, is a new mineral species from Temple Mountain, Emery County, Utah, U.S.A. It occurs as blue-green crusts and efflorescences in fractures in a fossil (Triassic) tree; individual crystals are <<1 mm and are intimately intergrown. Bobjonesite hydrates very easily, and is unstable in all but the driest atmosphere. Its structure was determined on a crystal of bobjonesite; however, the physical properties, optical properties and X-ray powder-diffraction pattern were recorded on the synthetic equivalent, and an electron-microprobe analysis was not possible. Bobjonesite has a pale blue streak, a vitreous luster and no observable fluorescence under ultraviolet light. It has no cleavage or parting. The Mohs hardness is ~1, and the calculated density is 2.28 g/cm3. Bobjonesite is biaxial positive, with \u03b1 1.555(2), \u03b2 1.561(1), \u03b3 1.574(2), 2V(obs.) = 72(1)\u00b0, 2V(calc.) = 69\u00b0; it is non-pleochroic,\u00a0X\u00a0=\u00a0b,\u00a0Y\u00a0\u2248\u00a0a,\u00a0Z\u00a0\u2227\u00a0c\u00a0\u2248 19\u00b0 (in \u03b2 obtuse). Bobjonesite is monoclinic, space group\u00a0P21/n, cell dimensions from single-crystal data:\u00a0a\u00a07.3940(5),\u00a0b\u00a07.4111(3),\u00a0c\u00a012.0597(9) A\u030a, \u03b2 106.55(1)\u00b0,\u00a0V\u00a0633.5(1) A\u030a3,\u00a0Z\u00a0= 4. The strongest seven lines in the X-ray powder-diffraction pattern [d\u00a0in A\u030a(I)(hkl)] are as follows: 5.795(100)(002), 3.498(90)(112), 3.881(48)(1\u030503), 5.408(37) (101), 4.571(20)(012), 6.962(11)(1\u030501) and 6.254(11)(011). The chemical formula was derived from crystal-structure analysis; the end-member formula is V O (SO4) (H2O)3. The crystal structure of bobjonesite was refined to an\u00a0R\u00a0index of 3.6% for 1105 observed (|\u00a0Fo\u00a0| > 5>F) reflections measured with an automated four-circle X-ray diffractometer using MoK\u03b1 X-radiation. There is one\u00a0V\u00a0site occupied by V4+\u00a0and surrounded by three O atoms and three (H2O) groups in an octahedral arrangement, with one short vanadyl bond (1.577 A\u030a), four similar equatorial bonds (<2.022 A\u030a>), and one longer V\u2013O bond (2.278 A\u030a)\u00a0trans\u00a0to the vanadyl bond. The structure consists of isolated [V4+2\u00a0O2\u00a0(H2O)6\u00a0(SO4)2] clusters linked by hydrogen bonds.",
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