Item talk:Q251047
From geokb
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"name": "40Ar* loss in experimentally deformed muscovite and biotite with implications for 40Ar/39Ar geochronology of naturally deformed rocks",
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"abstract": "The effects of deformation on radiogenic argon (40Ar\u2217) retentivity in mica are described from high pressure experiments performed on rock samples of peraluminous granite containing euhedral muscovite and biotite. Cylindrical cores, \u223c15\u00a0mm in length and 6.25\u00a0mm in diameter, were drilled from granite collected from the South Armorican Massif in northwestern France, loaded into gold capsules, and weld-sealed in the presence of excess water. The samples were deformed at a pressure of 10\u00a0kb and a temperature of 600\u00a0\u00b0C over a period 29 of hours within a solid medium assembly in a Griggs-type triaxial hydraulic deformation apparatus. Overall shortening in the experiments was approximately 10%. Transmitted light and secondary and backscattered electron imaging of the deformed granite samples reveals evidence of induced defects and for significant physical grain size reduction by kinking, cracking, and grain segmentation of the micas.Infrared (IR) laser (CO2) heating of individual 1.5\u20132.5\u00a0mm diameter grains of muscovite and biotite separated from the undeformed granite yield well-defined\u00a040Ar/39Ar plateau ages of 311\u00a0\u00b1\u00a02\u00a0Ma (2\u03c3). Identical experiments on single grains separated from the experimentally deformed granite yield results indicating\u00a040Ar\u2217\u00a0loss of 0\u201335% in muscovite and 2\u20133%\u00a040Ar\u2217\u00a0loss in biotite. Intragrain\u00a0in situ\u00a0ultraviolet (UV) laser ablation\u00a040Ar/39Ar ages (\u00b14\u201310%, 1\u03c3) of deformed muscovites range from 309\u00a0\u00b1\u00a013 to 264\u00a0\u00b1\u00a07\u00a0Ma, consistent with 0\u201316%\u00a040Ar\u2217\u00a0loss relative to the undeformed muscovite. The\u00a0in situ\u00a0UV laser ablation\u00a040Ar/39Ar ages of deformed biotite vary from 301 to 217\u00a0Ma, consistent with up to 32%\u00a040Ar\u2217\u00a0loss. No spatial correlation is observed between\u00a0in situ\u00a040Ar/39Ar age and position within individual grains. Using available argon diffusion data for muscovite the observed\u00a040Ar\u2217\u00a0loss in the experimentally treated muscovite can be utilized to predict average\u00a040Ar\u2217\u00a0diffusion dimensions. Maximum\u00a040Ar/39Ar ages obtained by UV laser ablation overlap those of the undeformed muscovite, indicating argon loss of <1% and an average effective grain radius for\u00a040Ar\u2217\u00a0diffusion \u2a7e700\u00a0\u03bcm. The UV laser ablation and IR laser incremental\u00a040Ar/39Ar ages indicating\u00a040Ar\u2217\u00a0loss of 16% and 35%, respectively, are consistent with an average diffusion radius \u226a100\u00a0\u03bcm. These results support a hypothesis of grain-scale\u00a040Ar\u2217\u00a0diffusion distances in undeformed mica and a heterogeneous mechanical reduction in the intragrain effective diffusion length scale for\u00a040Ar\u2217\u00a0in deformed mica. Reduction in the effective diffusion length scale in naturally deformed samples occurs most probably through production of mesoscopic and submicroscopic defects such as, e.g., stacking faults. A network of interconnected defects, continuously forming and annealing during dynamic deformation likely plays an important role in controlling both\u00a040Ar\u2217\u00a0retention and intragrain distribution in deformed mica. Intragrain\u00a040Ar/39Ar ages, when combined with estimates of diffusion kinetics and distances, may provide a means of establishing thermochronological histories from individual micas.",
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