{
"USGS Publications Warehouse": { "@context": "https://schema.org", "@type": "Article", "additionalType": "Journal Article", "name": "Spectrophotometric determination of fluorine in silicate rocks", "identifier": [ { "@type": "PropertyValue", "propertyID": "USGS Publications Warehouse IndexID", "value": "70009991", "url": "https://pubs.usgs.gov/publication/70009991" }, { "@type": "PropertyValue", "propertyID": "USGS Publications Warehouse Internal ID", "value": 70009991 }, { "@type": "PropertyValue", "propertyID": "DOI", "value": "10.1016/0039-9140(64)80192-2", "url": "https://doi.org/10.1016/0039-9140(64)80192-2" }, { "@type": "PropertyValue", "propertyID": "ISSN", "value": "00399140" } ], "journal": { "@type": "Periodical", "name": "Talanta", "volumeNumber": "11", "issueNumber": "9" }, "inLanguage": "en", "isPartOf": [ { "@type": "CreativeWorkSeries", "name": "Talanta" } ], "datePublished": "1964", "dateModified": "2020-11-24", "abstract": "The rock powder is sintered with a sodium carbonate flux containing zinc oxide and magnesium carbonate, the sinter-cake leached with water and the resulting solution filtered. Fluorine is separated from the acidified filtrate by steam distillation and determined spectrophotometrically by means of a zirconium-SPADNS reagent. If a multiple-unit distillation apparatus is used, 12 determinations can be completed per man-day.", "description": "5 p.", "publisher": { "@type": "Organization", "name": "Elsevier" }, "author": [ { "@type": "Person", "name": "Smith, V. C.", "givenName": "V. C.", "familyName": "Smith" }, { "@type": "Person", "name": "Peck, L. C.", "givenName": "L. C.", "familyName": "Peck" } ] }, "OpenAlex": { "abstract_inverted_index": { "The": [ 0 ], "rock": [ 1 ], "powder": [ 2 ], "is": [ 3, 27, 50 ], "sintered": [ 4 ], "with": [ 5, 19 ], "a": [ 6, 42, 46 ], "sodium": [ 7, 119 ], "carbonate": [ 8, 117, 127 ], "flux": [ 9 ], "containing": [ 10 ], "zinc": [ 11, 124 ], "oxide": [ 12 ], "and": [ 13, 21, 36 ], "magnesium": [ 14 ], "carbonate,": [ 15 ], "the": [ 16, 22, 30 ], "sinter-cake": [ 17 ], "leached": [ 18 ], "water": [ 20 ], "resulting": [ 23 ], "solution": [ 24, 139 ], "filtered.": [ 25 ], "Fluorine": [ 26 ], "separated": [ 28 ], "from": [ 29 ], "acidified": [ 31 ], "filtrate": [ 32 ], "by": [ 33, 39 ], "steam": [ 34 ], "distillation": [ 35, 48, 151, 168 ], "determined": [ 37 ], "spectrophotometrically": [ 38 ], "means": [ 40 ], "of": [ 41 ], "zirconium-SPADNS": [ 43 ], "reagent.": [ 44 ], "If": [ 45 ], "multiple-unit": [ 47 ], "apparatus": [ 49 ], "used,": [ 51 ], "12": [ 52, 99, 175 ], "determinations": [ 53 ], "can": [ 54 ], "be": [ 55 ], "completed": [ 56 ], "per": [ 57 ], "man-day.": [ 58 ], "Das": [ 59 ], "gepulverte": [ 60 ], "Gestein": [ 61 ], "wird": [ 62, 85 ], "mit": [ 63, 74, 92 ], "einer": [ 64, 96 ], "Sodaschmelze": [ 65 ], "gesintert,": [ 66 ], "die": [ 67, 78 ], "Zinkoxyd": [ 68 ], "und": [ 69, 77, 90, 103 ], "Magnesiumcarbonat": [ 70 ], "enth\u00e4lt,": [ 71 ], "der": [ 72 ], "Sinterkuchen": [ 73 ], "Wassen": [ 75 ], "ausgelaugt": [ 76 ], "L\u00f6sung": [ 79 ], "filtriert.": [ 80 ], "Aus": [ 81 ], "dem": [ 82 ], "anges\u00e4uerten": [ 83 ], "Filtrat": [ 84 ], "Fluor": [ 86 ], "durch": [ 87 ], "Wasserdampfdestillation": [ 88 ], "abgetrennt": [ 89 ], "spektralphotometrisch": [ 91 ], "Zirkonium-SPADNS": [ 93 ], "bestimmt.": [ 94 ], "Mit": [ 95 ], "Mehriachdestillationsapparatur": [ 97 ], "k\u00f6nnen": [ 98 ], "Bestimmungen": [ 100 ], "pro": [ 101 ], "Mann": [ 102 ], "Tag": [ 104 ], "gemacht": [ 105 ], "werden.": [ 106 ], "La": [ 107 ], "poudre": [ 108 ], "de": [ 109, 118, 121, 123, 128, 167, 179 ], "roche": [ 110 ], "est": [ 111, 133, 141 ], "fritt\u00e9e": [ 112, 132 ], "avec": [ 113 ], "un": [ 114, 159, 165 ], "fondant": [ 115 ], "au": [ 116 ], "contenant": [ 120 ], "l'oxyde": [ 122 ], "et": [ 125, 137, 155 ], "du": [ 126, 147 ], "magn\u00e9sium,": [ 129 ], "la": [ 130, 138, 153 ], "masse": [ 131 ], "lixivi\u00e9e": [ 134 ], "\u00e0": [ 135, 152, 169 ], "l'eau,": [ 136 ], "r\u00e9sultante": [ 140 ], "filtr\u00e9e.": [ 142 ], "On": [ 143 ], "s\u00e9pare": [ 144 ], "le": [ 145 ], "fluor": [ 146 ], "filtrat": [ 148 ], "acidifi\u00e9": [ 149 ], "par": [ 150, 158, 177 ], "vapeur,": [ 154 ], "dose": [ 156 ], "spectrophotom\u00e9triquement": [ 157 ], "r\u00e9actif": [ 160 ], "zirconium-SPADNS.": [ 161 ], "Si": [ 162 ], "l'on": [ 163 ], "utilise": [ 164 ], "appareil": [ 166 ], "unit\u00e9s": [ 170 ], "multiples,": [ 171 ], "on": [ 172 ], "peut": [ 173 ], "effectuer": [ 174 ], "dosages": [ 176 ], "journ\u00e9e": [ 178 ], "travail.": [ 180 ] }, "apc_list": { "value": 4130, "currency": "USD", "value_usd": 4130, "provenance": "doaj" }, "apc_paid": null, "authorships": [ { "author_position": "first", "author": { "id": "https://openalex.org/A5022003286", "display_name": "Lee C. Peck", "orcid": null }, "institutions": [ { "id": "https://openalex.org/I1286329397", "display_name": "United States Geological Survey", "ror": "https://ror.org/035a68863", "country_code": "US", "type": "government", "lineage": [ "https://openalex.org/I1286329397", "https://openalex.org/I1335927249" ] } ], "countries": [ "US" ], "is_corresponding": false, "raw_author_name": "Lee C. Peck", "raw_affiliation_strings": [ "U.S. Geological Survey, Denver 25, Colorado, U.S.A." ], "affiliations": [ { "raw_affiliation_string": "U.S. Geological Survey, Denver 25, Colorado, U.S.A.", "institution_ids": [ "https://openalex.org/I1286329397" ] } ] }, { "author_position": "last", "author": { "id": "https://openalex.org/A5037194125", "display_name": "Vertie C. Smith", "orcid": null }, "institutions": [ { "id": "https://openalex.org/I1286329397", "display_name": "United States Geological Survey", "ror": "https://ror.org/035a68863", "country_code": "US", "type": "government", "lineage": [ "https://openalex.org/I1286329397", "https://openalex.org/I1335927249" ] } ], "countries": [ "US" ], "is_corresponding": false, "raw_author_name": "Vertie C. Smith", "raw_affiliation_strings": [ "U.S. Geological Survey, Denver 25, Colorado, U.S.A." ], "affiliations": [ { "raw_affiliation_string": "U.S. Geological Survey, Denver 25, Colorado, U.S.A.", "institution_ids": [ "https://openalex.org/I1286329397" ] } ] } ], "best_oa_location": null, "biblio": { "volume": "11", "issue": "9", "first_page": "1343", "last_page": "1347" }, "citation_normalized_percentile": { "value": 0.942977, "is_in_top_1_percent": false, "is_in_top_10_percent": true }, "cited_by_api_url": "https://api.openalex.org/works?filter=cites:W2084406878", "cited_by_count": 26, "cited_by_percentile_year": { "min": 92, "max": 93 }, "concepts": [ { "id": "https://openalex.org/C185592680", "wikidata": "https://www.wikidata.org/wiki/Q2329", "display_name": "Chemistry", "level": 0, "score": 0.9554001 }, { "id": "https://openalex.org/C13965031", "wikidata": "https://www.wikidata.org/wiki/Q243545", "display_name": "Nuclear chemistry", "level": 1, "score": 0.5710582 }, { "id": "https://openalex.org/C2778657360", "wikidata": "https://www.wikidata.org/wiki/Q190227", "display_name": "Sodium carbonate", "level": 3, "score": 0.5679942 }, { "id": "https://openalex.org/C204030448", "wikidata": "https://www.wikidata.org/wiki/Q101017", "display_name": "Distillation", "level": 2, "score": 0.5267909 }, { "id": "https://openalex.org/C2780659211", "wikidata": "https://www.wikidata.org/wiki/Q181699", "display_name": "Carbonate", "level": 2, "score": 0.45835415 }, { "id": "https://openalex.org/C537181965", "wikidata": "https://www.wikidata.org/wiki/Q658", "display_name": "Sodium", "level": 2, "score": 0.3216011 }, { "id": "https://openalex.org/C43617362", "wikidata": "https://www.wikidata.org/wiki/Q170050", "display_name": "Chromatography", "level": 1, "score": 0.23844042 }, { "id": "https://openalex.org/C178790620", "wikidata": "https://www.wikidata.org/wiki/Q11351", "display_name": "Organic chemistry", "level": 1, "score": 0.07651192 } ], "corresponding_author_ids": [], "corresponding_institution_ids": [], "countries_distinct_count": 1, "counts_by_year": [ { "year": 2018, "cited_by_count": 1 } ], "created_date": "2016-06-24", "datasets": [], "display_name": "Spectrophotometric determination of fluorine in silicate rocks", "doi": "https://doi.org/10.1016/0039-9140(64)80192-2", "fulltext_origin": "ngrams", "fwci": 3.87, "grants": [], "has_fulltext": true, "id": "https://openalex.org/W2084406878", "ids": { "openalex": "https://openalex.org/W2084406878", "doi": "https://doi.org/10.1016/0039-9140(64)80192-2", "mag": "2084406878" }, "indexed_in": [ "crossref" ], "institutions_distinct_count": 1, "is_paratext": false, "is_retracted": false, "keywords": [ { "id": "https://openalex.org/keywords/sodium-carbonate", "display_name": "Sodium carbonate", "score": 0.5679942 }, { "id": "https://openalex.org/keywords/defluoridation", "display_name": "Defluoridation", "score": 0.539562 } ], "language": "fr", "locations": [ { "is_oa": false, "landing_page_url": "https://doi.org/10.1016/0039-9140(64)80192-2", "pdf_url": null, "source": { "id": "https://openalex.org/S124795565", "display_name": "Talanta", "issn_l": "0039-9140", "issn": [ "0039-9140", "1873-3573" ], "is_oa": false, "is_in_doaj": false, "is_core": true, "host_organization": "https://openalex.org/P4310320990", "host_organization_name": "Elsevier BV", "host_organization_lineage": [ "https://openalex.org/P4310320990" ], "host_organization_lineage_names": [ "Elsevier BV" ], "type": "journal" }, "license": null, "license_id": null, "version": null, "is_accepted": false, "is_published": false } ], "locations_count": 1, "mesh": [], "ngrams_url": "https://api.openalex.org/works/W2084406878/ngrams", "open_access": { "is_oa": false, "oa_status": "closed", "oa_url": null, "any_repository_has_fulltext": false }, "primary_location": { "is_oa": false, "landing_page_url": "https://doi.org/10.1016/0039-9140(64)80192-2", "pdf_url": null, "source": { "id": "https://openalex.org/S124795565", "display_name": "Talanta", "issn_l": "0039-9140", "issn": [ "0039-9140", "1873-3573" ], "is_oa": false, "is_in_doaj": false, "is_core": true, "host_organization": "https://openalex.org/P4310320990", "host_organization_name": "Elsevier BV", "host_organization_lineage": [ "https://openalex.org/P4310320990" ], "host_organization_lineage_names": [ "Elsevier BV" ], "type": "journal" }, "license": null, "license_id": null, "version": null, "is_accepted": false, "is_published": false }, "primary_topic": { "id": "https://openalex.org/T10180", "display_name": "Analytical Chemistry Techniques", "score": 0.953, "subfield": { "id": "https://openalex.org/subfields/1602", "display_name": "Analytical Chemistry" }, "field": { "id": "https://openalex.org/fields/16", "display_name": "Chemistry" }, "domain": { "id": "https://openalex.org/domains/3", "display_name": "Physical Sciences" } }, "publication_date": "1964-09-01", "publication_year": 1964, "referenced_works": [ "https://openalex.org/W1973076235", "https://openalex.org/W1982211974", "https://openalex.org/W2058074580" ], "referenced_works_count": 3, "related_works": [ "https://openalex.org/W4246956788", "https://openalex.org/W3149668185", "https://openalex.org/W3034403885", "https://openalex.org/W3026162553", "https://openalex.org/W2890927948", "https://openalex.org/W2589119674", "https://openalex.org/W2074407759", "https://openalex.org/W2067757873", "https://openalex.org/W2005654684", "https://openalex.org/W1594482144" ], "sustainable_development_goals": [], "title": "Spectrophotometric determination of fluorine in silicate rocks", "topics": [ { "id": "https://openalex.org/T10180", "display_name": "Analytical Chemistry Techniques", "score": 0.953, "subfield": { "id": "https://openalex.org/subfields/1602", "display_name": "Analytical Chemistry" }, "field": { "id": "https://openalex.org/fields/16", "display_name": "Chemistry" }, "domain": { "id": "https://openalex.org/domains/3", "display_name": "Physical Sciences" } }, { "id": "https://openalex.org/T13563", "display_name": "Perchlorate Contamination and Health Effects", "score": 0.9454, "subfield": { "id": "https://openalex.org/subfields/2307", "display_name": "Health, Toxicology and Mutagenesis" }, "field": { "id": "https://openalex.org/fields/23", "display_name": "Environmental Science" }, "domain": { "id": "https://openalex.org/domains/3", "display_name": "Physical Sciences" } }, { "id": "https://openalex.org/T11969", "display_name": "Fluoride Contamination in Drinking Water and Defluoridation Methods", "score": 0.9191, "subfield": { "id": "https://openalex.org/subfields/2312", "display_name": "Water Science and Technology" }, "field": { "id": "https://openalex.org/fields/23", "display_name": "Environmental Science" }, "domain": { "id": "https://openalex.org/domains/3", "display_name": "Physical Sciences" } } ], "type": "article", "type_crossref": "journal-article", "updated_date": "2024-08-13T15:04:03.433766", "versions": [] }
}